{"product_id":"operando-xrd-ec-h-cell-min-2-of-5","title":"Operando XRD EC H-Cell, min 2θ of 5°","description":"\u003cp\u003eThis is a vertically mounted electrochemical cell for operando goniometric X-Ray Diffraction (XRD) during the electrochemical experiment. The cell can be used as a two-compartment H-cell with the working electrode and the counter electrode separated by a membrane, or it can be used without a membrane as a single-compartment cell. The working electrode is mounted on a height adjustable centre post and can accept samples up to 25 mm x 25 mm and up to 4 mm thick. By using interchangeable adapters, the cell can work with different sample sizes (one adapter included). Electrical contact to the working electrode is made via a “wet” tantalum foil which, with the Kapton foil window, determines the electrolyte thickness, standard is 300 µm. This allows for lower energy X-Ray sources to be used to perform measurements with a minimum 2θ of 5°. The cell can be used in both flow and stagnant mode, in each chamber independently.\u003c\/p\u003e\n\u003cp\u003eThe cell consists of a multipart PEEK body with a separable compartment for the counter electrode for either single or double compartment operation depending on whether or not a membrane is installed. Both compartments are fitted with tubing for independent electrolyte filling and recirculation. The working electrode is placed on a pedestal which is inserted into the bottom of the cell, and can be translated along the vertical axis using a set screw so that the active surface of the working electrode is placed in contact with the tantalum foil, which together with the Kapton film window is secured to the cell body via a polished stainless steel flange and screws. It accepts our standard 6 mm reference electrodes, as well as 6 mm diameter rod or helix counter electrodes. It is available in two variants, for aqueous or organic electrolytes, with FKM\/EPDM or FFKM O-Rings, respectively. When properly assembled and maintained, the cell is gas- and liquid-tight.\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eApplication note\u003cbr\u003e\u003c\/strong\u003eThis XRD EC H-cell is optimised for demanding operando electrochemical and XRD experiments. The minimum electrolyte thickness and geometry allow for real-time measurements of ion intercalation in electrochemically active materials or monitor the progress of electrochemical processing (deposition etc.) using either low or high energy X-ray sources with a minimum 2θ value of 5°. It is compatible with most goniometric XRD instruments and can be customised on request. For troubleshooting instruction see the \u003cspan\u003e blog post\u003c\/span\u003e\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eSpecification\u003cbr\u003e\u003c\/strong\u003eelectrolyte thickness: 300 µm\u003cbr\u003eminimum 2θ: 5°\u003cbr\u003eWE chamber volume: ~10 mL\u003cbr\u003eCE chamber volume: ~2 mL\u003cbr\u003emaximum WE thickness: 4 mm\u003cbr\u003eWE size: 7x7, 10x10, 15x15, or 25x25 mm\u003csup\u003e2\u003c\/sup\u003e\u003cbr\u003eelectrode plug diameter: 6 mm\u003cbr\u003emembrane active area: 1cm\u003csup\u003e2\u003c\/sup\u003e\u003cbr\u003erecommended membrane diameter: 20 mm\u003cbr\u003eminimum membrane diameter: 16 mm\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eIntrastat data\u003c\/strong\u003e\u003cbr\u003eHS Code: 90275000 \u003cbr\u003eCountry of Origin: Sweden \u003cbr\u003eNET weight: 100g\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eProduct includes\u003cbr\u003e\u003c\/strong\u003e1 x WE chamber\u003cbr data-mce-fragment=\"1\"\u003e1 x CE chamber\u003cbr data-mce-fragment=\"1\"\u003e1 x clam screw\u003cbr data-mce-fragment=\"1\"\u003e1 x sampel size adapter\u003cbr data-mce-fragment=\"1\"\u003e1 x WE plunger\u003cbr data-mce-fragment=\"1\"\u003e1 x SS16L window holder\u003cbr data-mce-fragment=\"1\"\u003e1 x set of SS16L screws (window holder)\u003cbr data-mce-fragment=\"1\"\u003e1 x set of PEEK screws (WE\/CE compartment)\u003cbr data-mce-fragment=\"1\"\u003e1 x set of Nylon screws (cell holder)\u003cbr data-mce-fragment=\"1\"\u003e1 x tantalum wet contact\u003cbr data-mce-fragment=\"1\"\u003e1 x set of Kapton windows (5 pcs)\u003cbr data-mce-fragment=\"1\"\u003e1 x cell holder (variant dependent)\u003cbr data-mce-fragment=\"1\"\u003e1 x set of O-Rings\u003cbr data-mce-fragment=\"1\"\u003e1 x window gasket\u003cbr\u003e1 x plug\u003cbr\u003e1 x Metal Wire Auxiliary Electrode - 35HX15 0.6\/235 mm\u003cbr\u003e1 x Ag\/AgCl or Ag\/Ag+ reference electrode\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eRelated products\u003cbr\u003e\u003c\/strong\u003eBEC 50 mL - Basic Electrochemical Cell\u003cspan data-mce-fragment=\"1\"\u003e\u003cbr data-mce-fragment=\"1\"\u003ePeristaltic pump\u003c\/span\u003e\u003cbr\u003e\u003c\/p\u003e","brand":"redox.me","offers":[{"title":"water-based electrolyte \/ 10 mm x 10 mm (default) \/ BRUKER AXS XRD Diffractometer","offer_id":56885661630790,"sku":"C-A-OPT_XRD_HC-10x10-BRU","price":6481.0,"currency_code":"EUR","in_stock":true},{"title":"water-based electrolyte \/ 10 mm x 10 mm (default) \/ Malvern Panalytical XRD Diffractometer","offer_id":56885661663558,"sku":"C-A-OPT_XRD_HC-10x10-PAN","price":6481.0,"currency_code":"EUR","in_stock":true},{"title":"water-based electrolyte \/ 10 mm x 10 mm (default) \/ Rigaku XRD Diffractometer","offer_id":56885661696326,"sku":"C-A-OPT_XRD_HC-10x10-RIG","price":6481.0,"currency_code":"EUR","in_stock":true},{"title":"water-based electrolyte \/ 25 mm x 25 mm \/ BRUKER AXS XRD 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